RUBIDIUM β-DIKETONATES

Rubidium β-diketonates were proposed as potential precursors for the growth of Rb-containing thin films by MOCVD or ALD. [[i]]

 [i] R. G. Gordon, US Patent US 6,258,157 B1, Jul. 10, 2001

https://patentimages.storage.googleapis.com/10/ac/b4/c1fe802fa1385d/US6258157.pdf

Rubidium acetylacetonate Rb(acac)

    Rubidium (I) acetylacetonate (or rubidium 2,4-pentanedionate) Rb(acac) (RbC5H7O2, M= 184.58) was synthesized and characterized. Rb(acac) is white solid , having melting point 200°C. [i]

Evidence for strong ion association/ ion-pair formation in Rb(acac) was revealed. (same as in analogous Li, Na, K and Cs acetylacetonates).[[ii]

[i] https://www.americanelements.com/rubidium-acetylacetonate-66169-93-5

[ii] C.R. Bhattacharjee, M. Bhattacharjee ; M.K. Chaudhuri, H. Sangchungnunga, J. Chem. Res. Synopses, 1991, no9, pp. 250-251 “ First synthesis of (acetylacetonato)rubidium(I), a direct route to (acetylacetonato)caesium(I) and evidence for strong ion association/ion-pair formation in M(acac) (M=Li, Na, K, Rb or Cs)”

Rubidium 2,2,6,6-tetramethylheptane-3,5-dionate Rb(thd)

Rubidium 2,2,6,6-tetramethylheptane-3,5-dionate Rb(thd) (Rb(C11H19O2, M=268.74) is white to off-white powder.  [[i]]

Rb(thd) was found to be completely insoluble in in supercritical CO2 (0 mol/L) under these conditions: 100-200bar/ 60°C  [ii]

[ii]    O. Aschenbrenner,  S. Kemper,  N. Dahmen,  K. Schaber,  E. Dinjus, J. Supercritical Fluids, 2007, Vol.41, Iss.2, p. 179–186, “Solubility of β-diketonates, cyclopentadienyls, and cyclooctadiene complexes with various metals in supercritical carbon dioxide”

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