ZIRCONIUM CYCLOPENTADIENYLS-TETRAHYDROBORATES

Zirconium (cyclopentadienyl) tris(tetrahydroborate) Zr(Cp)(BH4)3, Zirconium bis(cyclopentadienyl) bis(tetrahydroborate) Zr(Cp)2(BH4)2

Zirconium (cyclopentadienyl) tris(tetrahydroborate) Zr(Cp)(BH4)3 and Zirconium bis(cyclopentadienyl) bis(tetrahydroborate) Zr(Cp)2(BH4)2 were used as precursors for the CVD growth of  thin films of zirconium carbide-boride ZrCxBy as well as zirconium carbide ZrCx at temperatures 300–600°C for hard coating applications. Mass spectrometry fragmentation patterns were studied to rationalize trends in the deposition temperature and chemical composition of the obtained thin films. [[i]]

 [i] K. Hankó, G. Vass, L. Szepes, J. Organomet. Chem., 1995, Vol.492, Iss2, p.235-239, ”Arene-transition metal complexes as precursors of hard coatings prepared by the chemical vapour deposition technique

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